A new assembling method to sinter pure PcBN material
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摘要: 为降低合成纯PcBN的温度和压力条件,改进合成腔体内的组装方式:使用横截面积更小的高导电型石墨管,采用双加热管设计和填充大尺寸的白云石。采用新型组装方式,在高温超高压条件下用粒度尺寸为10 μm的cBN的微粉合成出纯聚晶立方氮化硼(PcBN)烧结体。利用扫描电子显微镜(SEM)、X射线衍射仪(XRD)对烧结体的微观形貌和物相进行分析,同时测试烧结体的致密性、显微硬度以及抗压强度。结果表明:采用新型组装方式可在相对较低的烧结温度下得到性能良好的纯PcBN样品。在压力为7.5 GPa,温度为1 700 ℃下烧结得到的纯PcBN的组织结构致密度最好,其硬度达到了3 992.7 Hv,高于传统PcBN材料的硬度,且样品中形成大量的cBN-cBN颗粒间键合,有效提升了烧结体的综合性能。Abstract: A new assembling method was used in pure polycrystalline cubic boron nitride (PcBN) HPHT synthesis chamber. The cBN powder with particle size of 10 μm was used as the raw material. Scanning electron microscope (SEM) and X-ray diffraction (XRD) were used to analyze the microstructure and the phase of the sintered body, and the compactness, the microhardness and the compressive strength were tested as well. Results show that pure PcBN with good properties could be obtained at a relatively lower sintering temperature by using this new assembly method. It is also found that the sample sintered at 7.5 GPa and 1 700 ℃ has the best microstructure density and that its hardness reached 3 992.7 Hv, which is higher than that of the traditional PcBN material. A large number of cBN-cBN particle bonds were formed in the sample, which effectively improves the comprehensive properties of the sintered body.
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Key words:
- pure PcBN /
- assembly method /
- high temperature and high pressure /
- hardness
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