Effect of particle size and content of silicon powder on microstructure and properties of SiC ceramic materials
-
摘要: 将平均粒径为75 μm和48 μm、质量分数为0%~8%的Si粉分别添加到SiC陶瓷材料中,在1550℃下保温3 h烧成,研究Si粉粒径及其添加量对SiC陶瓷材料烧结性能、力学性能和显微结构的影响。结果表明:添加不同粒径及质量分数的Si粉可改善SiC陶瓷材料的显微结构,提高其烧结性能和力学性能;在一定范围内,较小粒径的Si粉更有利于形成均匀、致密的SiC烧结体,大幅提升SiC陶瓷材料的性能;当Si粉粒径为48 μm且添加的质量分数为4%时,SiC陶瓷材料的烧结性能和力学性能较优,其体积密度和显气孔率分别为2.58 g/cm3和13.5%,抗弯强度和洛氏硬度分别为25 MPa和115 HRB。Abstract: Si powders with average particle sizes of 75 μm and 48 μm respectively and mass fraction from 0% to 8% were added to the SiC ceramic materials which were sintered at 1550℃ for 3 h. The effects of particle size and addition amount of Si powder on sintering properties, mechanical properties and microstructures of SiC ceramics were studied. The results show that the addition of Si powder with different particle size and content can improve the microstructure of SiC ceramic material and improve its sintering and mechanical properties. Within a certain range, the smaller particle size of Si powder is more conducive to the formation of uniform and compact SiC sintered body, and greatly improves the performance of SiC ceramic material. When the particle size of Si powder is 48 μm and the mass fraction is 4%, the sintering and mechanical properties of SiC ceramics are better, whose volume density and apparent porosity are 2.58 g/cm3 and 13.5% respectively, with flexural strength and hardness 25 MPa and 115 HRB respectively.
-
Key words:
- SiC ceramic material /
- sintering property /
- Si powder /
- mechanical property /
- microstructure
点击查看大图
计量
- 文章访问数: 189
- HTML全文浏览量: 40
- PDF下载量: 7
- 被引次数: 0