Research on the interface relation between TiN0.3/AlN and CBN in PCBN sintering body
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摘要: 针对传统结合剂的PCBN超硬刀具材料在无液干切削过程中存在耐热性不足、软点等问题,采用非化学计量比TiN0.3与AlN为结合剂的方法制备PCBN。使用SEM、XRD、EDS、DIL膨胀仪及硬度测量设备,对样品的抛光表面和断口进行观察,样品相组成分析,界面处的元素分布,膨胀系数及硬度等方面的分析,讨论TiN0.3与CBN及TiN0.3/AlN与CBN表面的结合状态,分析TiN与CBN热膨胀系数的差异,及这种差异对烧结体组织的影响。引入AlN减轻膨胀系数的影响;通过CBN表面镀钛,使TiN0.3、TiN0.3/AlN与CBN更好结合。分析CBN表面区域与TiN0.3、TiN0.3/AlN的生成物,并且分析这些生成物在PCBN中的作用。
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关键词:
- PCBN /
- TiN0.3/AlN结合剂 /
- 界面关系
Abstract: To solve the problems in dry cutting with traditional bond polycrystalline cubic boron nitride(PCBN),such as low heat resistance,non-stoichiometric ration TiN0.3 is used to prepare new bonding system of PCBN.SEM,XRD and EDS are used to observe the polished surface and fracture of the samples,as well as the components and element distribution at the interface,thus analyzing bonding status of TiN0.3 to CBN and TiN0.3/AlN to CBN.Expansion coefficient and hardness are tested using DIL and FM equipment to discuss the difference between thermal expansion coefficients of TiN and CBN and the effect of this difference on the sintered body.Furthermore,AlN is introduced to reduce the effect of expansion coefficient.After coating Ti on CBN surface,TiN0.3 and TiN0.3/AlN are better bonded with CBN.The resultant at the interface of CBN to TiN0.3 or TiN0.3/AlN are analyzed,as well as its function in PCBN.
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